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Beilstein J. Org. Chem. 2015, 11, 1547–1552, doi:10.3762/bjoc.11.170
Graphical Abstract
Figure 1: Proposed structure of GnTs inhibitors.
Scheme 1: Reagents and conditions: a) MsCl, Et3N, CH2Cl2, 0 °C → rt, overnight, 93%; b) NaN3, H2O/DMF 1:20 (v...
Scheme 2: Reagents and conditions: a) H2SO4, MeOH, rt, overnight, 71%; b) H2SO4, 70% AcOH, 0 °C → rt, 4 h, 84...
Figure 2: Molecular structure (ORTEP drawing with adjacent ChemDraw image) of compound 12. Atomic displacemen...
Scheme 3: Reagents and conditions: a) EtSH, BF3·OEt2, CH2Cl2, −5 °C → rt, 4 h, 13: 55%, 14: 34%.